A novel spectrophotometric method based on Seliwanoff test to determine 5-(Hydroxymethyl) furfural (HMF) in honey: Development, in house validation and application
Yazarlar (4)
Arş. Gör. Ayşegül Beşir Özgeçen Ondokuz Mayis Üniversitesi, Türkiye
Prof. Dr. Fehmi Yazıcı Ondokuz Mayis Üniversitesi, Türkiye
Doç. Dr. Mustafa Mortaş Ondokuz Mayis Üniversitesi, Türkiye
Prof. Dr. Osman GÜL Kastamonu Üniversitesi, Türkiye
| Makale Türü | Özgün Makale (SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale) | ||
| Dergi Adı | Lwt (Q1) | ||
| Dergi ISSN | 0023-6438 Wos Dergi Scopus Dergi | ||
| Dergi Tarandığı Indeksler | SCI-Expanded | ||
| Makale Dili | Türkçe | Basım Tarihi | 01-2021 |
| Kabul Tarihi | – | Yayınlanma Tarihi | 01-03-2021 |
| Cilt / Sayı / Sayfa | 139 / 1 / – | DOI | 10.1016/j.lwt.2020.110602 |
| Makale Linki | http://dx.doi.org/10.1016/j.lwt.2020.110602 | ||
| Özet |
| A new spectrophotometric method for the determination of 5-(Hydroxymethyl) furfural (5-HMF) in honey was proposed. In the proposed method based on the qualitative Seliwanoff test, quantitative determination was carried out by measuring the red color formed by reacting the HMF and Seliwanoff reagent (resorcinol-HCl). Central Composite Design (CCD) was used to obtain optimum reaction parameters. The limit of detection, LOD (2.69 mg kg−1) and limit of quantification, LOQ (8.97 mg kg−1) were established in the model honey matrix. Precision (as RSD for inter and intraday precision) was in the range of 2.52–5.14%. Accuracy results obtained exhibit a good recovery (from 95.83% to 96.65%). Good selectivity and linearity (R2 > 0.99) were also observed. HMF amounts in honey samples determined by the proposed method were found to be in a relatively good agreement with those obtained by the … |
| Anahtar Kelimeler |
| Hydroxymethylfurfural | Quantitative | Seliwanoff test | Spectrophotometric | Validation |
Science Direct
A novel spectrophotometric method based on Seliwanoff test to determine 5-(Hydroxymethyl) furfural (HMF) in honey: Development, in house validation and application
BM Sürdürülebilir Kalkınma Amaçları
| Atıf Sayıları | |
| Scopus | 46 |
| Google Scholar | 64 |