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Crystal structure of (2E)-1-(4-hydroxyphenyl)-3-(4-methoxyphenyl)prop-2-en-1-one    
Yazarlar (5)
Fatma Yeşilyurt
Prof. Dr. Abdullah AYDIN Prof. Dr. Abdullah AYDIN
Kastamonu Üniversitesi, Türkiye
Halise İnci Gül
Atatürk Üniversitesi, Türkiye
Mehmet Akkurt
Erciyes Üniversitesi, Türkiye
Nefise Özçelik
Aksaray Üniversitesi, Türkiye
Devamını Göster
Özet
The compound, C 16 H 14 O 3,(except H atoms) is almost planar [rms deviations for all non-H atoms= 0.001 Å] and the dihedral angle between the aromatic rings is 9.35 (7). In the crystal, molecules are linked by intermolecular O—H··· O and C—H··· O hydrogen bonds, forming a three-dimensional network structure. Furthermore, a weak π-π stacking interactions [centroid-to-centroid distance= 3.7055 (9) Å] contributes to the stabilization of the molecular packing. Crystal Data for C 16 H 14 O 3 (M= 254.27 g/mol): Orthorhombic, space group Pbca (no. 61), a= 13.4563 (16) Å, b= 11.4986 (14) Å, c= 16.720 (2) Å, V= 2587.1 (5) Å 3, Z= 8, T= 296 (2) K, μ (MoKα)= 0.090 mm-1, D calc= 1.306 g/cm 3, 61402 reflections measured (4.88≤ 2Θ≤ 56.76), 3240 unique (R int= 0.0334, R sigma= 0.0120) which were used in all calculations. The final R 1 was 0.0438 (I≥ 2σ (I)) and wR 2 was 0.1228 (all data).
Anahtar Kelimeler
Makale Türü Özgün Makale
Makale Alt Türü Diğer hakemli uluslarası dergilerde yayınlanan tam makale
Dergi Adı European Journal of Chemistry
Dergi ISSN 2153-2257
Dergi Tarandığı Indeksler Index Copernicus
Makale Dili İngilizce
Basım Tarihi 01-2018
Cilt No 9
Sayı 2
Sayfalar 147 / 150
Doi Numarası 10.5155/eurjchem.9.2.147-150.1733
Makale Linki http://dx.doi.org/10.5155/eurjchem.9.2.147-150.1733
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Crystal structure of (2E)-1-(4-hydroxyphenyl)-3-(4-methoxyphenyl)prop-2-en-1-one

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