Yazarlar (5) |
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![]() Kastamonu Üniversitesi, Türkiye |
![]() Atatürk Üniversitesi, Türkiye |
![]() Erciyes Üniversitesi, Türkiye |
![]() Aksaray Üniversitesi, Türkiye |
Özet |
The compound, C 16 H 14 O 3,(except H atoms) is almost planar [rms deviations for all non-H atoms= 0.001 Å] and the dihedral angle between the aromatic rings is 9.35 (7). In the crystal, molecules are linked by intermolecular O—H··· O and C—H··· O hydrogen bonds, forming a three-dimensional network structure. Furthermore, a weak π-π stacking interactions [centroid-to-centroid distance= 3.7055 (9) Å] contributes to the stabilization of the molecular packing. Crystal Data for C 16 H 14 O 3 (M= 254.27 g/mol): Orthorhombic, space group Pbca (no. 61), a= 13.4563 (16) Å, b= 11.4986 (14) Å, c= 16.720 (2) Å, V= 2587.1 (5) Å 3, Z= 8, T= 296 (2) K, μ (MoKα)= 0.090 mm-1, D calc= 1.306 g/cm 3, 61402 reflections measured (4.88≤ 2Θ≤ 56.76), 3240 unique (R int= 0.0334, R sigma= 0.0120) which were used in all calculations. The final R 1 was 0.0438 (I≥ 2σ (I)) and wR 2 was 0.1228 (all data). |
Anahtar Kelimeler |
Makale Türü | Özgün Makale |
Makale Alt Türü | Diğer hakemli uluslarası dergilerde yayınlanan tam makale |
Dergi Adı | European Journal of Chemistry |
Dergi ISSN | 2153-2257 |
Dergi Tarandığı Indeksler | Index Copernicus |
Makale Dili | İngilizce |
Basım Tarihi | 01-2018 |
Cilt No | 9 |
Sayı | 2 |
Sayfalar | 147 / 150 |
Doi Numarası | 10.5155/eurjchem.9.2.147-150.1733 |
Makale Linki | http://dx.doi.org/10.5155/eurjchem.9.2.147-150.1733 |