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Synthesis, Crystal Structure and Spectroscopic Characterization of {6-[2-(2-chlorophenyl)-1,3-thiazol-4-yl]-2-oxo-1,3-benzothiazol-3(2H)-yl}acetic acid      
Yazarlar
Prof. Dr. Abdullah AYDIN Prof. Dr. Abdullah AYDIN
Kastamonu Üniversitesi, Türkiye
Mehmet Akkurt
Erciyes Üniversitesi, Türkiye
Leyla Uzun
Leyla Yıldırım
Türkiye
Tijen Önkol
Türkiye
Özet
The title compound {6-[2-(2-chlorophenyl)-1,3-thiazol-4-yl]-2-oxo-1,3- benzothiazol-3(2H)-yl}acetic acid was prepared and characterized by elemental analyses, FT-IR, 1 H NMR spectroscopy, X-ray diffraction. A quantum-chemical calculation was performed using the CNDO method. In the title compound, C 18 H 11 ClN 2 O 3 S 2 , the crystal structure is stabilized by intermolecular hydrogen bonds (C-H•••O=C) to form centrosymmetric R-{2}^{2} (16) dimers and the C-H•••O, O-H•••N, and C-H•••N interactions generating the graph set motifs R-{2}^{2} (9) and R-{2}^{2} (22). Index Abstract: [Figure not available: see fulltext.] © 2010 Springer Science+Business Media, LLC.
Anahtar Kelimeler
Acetic acid | CNDO method | Crystal structure | X-ray
Makale Türü Özgün Makale
Makale Alt Türü SSCI, AHCI, SCI, SCI-Exp dergilerinde yayımlanan tam makale
Dergi Adı JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
Dergi ISSN 1074-1542
Dergi Tarandığı Indeksler SCI-Expanded
Dergi Grubu Q4
Makale Dili İngilizce
Basım Tarihi 10-2010
Cilt No 40
Sayı 10
Sayfalar 816 / 820
Doi Numarası 10.1007/s10870-010-9744-4
Makale Linki http://dx.doi.org/10.1007/s10870-010-9744-4