Synthesis, spectral, and thermal characterisations of some azo-ester derivatives containing a 4-acryloyloxy group
Yazarlar (3)
Prof. Dr. Mahmut GÜR Kastamonu Üniversitesi, Türkiye
Prof. Dr. Hasan Kocaokutgen Ondokuz Mayıs Üniversitesi, Türkiye
Prof. Dr. Murat Taş Ondokuz Mayıs Üniversitesi, Türkiye
Makale Türü Özgün Makale (SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
Dergi Adı Dyes and Pigments
Dergi ISSN 0143-7208 Wos Dergi Scopus Dergi
Dergi Tarandığı Indeksler SCI
Makale Dili İngilizce Basım Tarihi 01-2007
Cilt / Sayı / Sayfa 72 / 1 / 101–108 DOI 10.1016/j.dyepig.2005.08.005
Makale Linki https://linkinghub.elsevier.com/retrieve/pii/S0143720805002597
UAK Araştırma Alanları
Organik Kimya
Özet
The azo-ester compounds containing an acryloyloxy group were derived from phenol and 2,6-dimethylphenol; first azobenzene derivatives were prepared by reacting substituted benzenediazonium salts with phenol and 2,6-dimethylphenol then their acryloyloxy derivatives were synthesized in a Schotten–Bauman-type reaction. The characterisation of the synthesized azo-ester dye has been described by IR, UV–vis, 1H NMR, 13C NMR spectroscopic techniques, and elemental analysis. The influence of the substituents and acryloyloxy group on the spectral data of the synthesized compounds has been described. The thermal behaviour of the present compounds has been determined by means of differential thermal analysis (DTA) and thermogravimetry (TG) techniques.
Anahtar Kelimeler
Acrylate | Acryloyloxy | Azo-ester dyes | Azobenzene | Diazenes | Spectral characterisation | Thermal analysis