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Experimental and theoretical approaches for electrical, magnetic, micromechanical, and structural characterization of BSCCO ceramic superconductors    
Yazarlar
Serap Safran
Ankara Üniversitesi, Türkiye
Ozturk Hamit
Fatih Bulut
Sinop Üniversitesi, Türkiye
Prof. Dr. Özgür ÖZTÜRK Prof. Dr. Özgür ÖZTÜRK
Kastamonu Üniversitesi, Türkiye
Özet
This study investigates how the preparation and re-pelletization of BSCCO ceramic superconductors affects their structural, magnetic, electrical, and mechanical properties. Samples were prepared using conventional methods including the dry solid state (SS) reaction and wet ammonium nitrate (AN) precipitation, with three variations prepared for each technique. The fabricated samples were then characterized with X-ray powder diffraction (XRD) and scanning electron microscopy. The density, resistance vs. temperature characteristics, AC susceptibility vs. temperature characteristics, and magnetic hysteresis properties were measured. In addition, Vicker's microhardness was measured and revealed that all six samples exhibit the reverse indentation size effect (RISE). Microhardness modeling was also conducted. Calculations with Meyer's law, the Hays and Kendall model, and the proportional sample resistance model indicate that the samples are far from the plateau region, whereas the indentation-induced cracking model was consistent with the experimental results. The elastic modulus, Young's modulus, yield strength, and brittleness index were also calculated for each sample.
Anahtar Kelimeler
Characterization | High-temperature superconductor | Production method | Re-pelletization | Theoretical approaches
Makale Türü Özgün Makale
Makale Alt Türü SSCI, AHCI, SCI, SCI-Exp dergilerinde yayımlanan tam makale
Dergi Adı Ceramics International
Dergi ISSN 0272-8842
Dergi Tarandığı Indeksler SCI-Expanded
Makale Dili İngilizce
Basım Tarihi 01-2018
Cilt No 44
Sayı 10
Sayfalar 11674 / 11681
Doi Numarası 10.1016/j.ceramint.2018.03.243