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Structural and mechanical characterization of Bi1 75Pb0 25Sr2Ca2Cu3 xSnxO10 y superconductor ceramics using Vickers microhardness test       
Yazarlar
Haluk Koralay
Gazi Üniversitesi, Türkiye
A Arslan
Şükrü Çavdar
Gazi Üniversitesi, Türkiye
Prof. Dr. Özgür ÖZTÜRK Prof. Dr. Özgür ÖZTÜRK
Kastamonu Üniversitesi, Türkiye
Doç. Dr. Elif AŞIKUZUN TOKEŞER Doç. Dr. Elif AŞIKUZUN TOKEŞER
Kastamonu Üniversitesi, Türkiye
Abdullah Günen
Gazi Üniversitesi, Türkiye
Prof. Dr. Ahmet Tolga TAŞÇI Prof. Dr. Ahmet Tolga TAŞÇI
Kastamonu Üniversitesi, Türkiye
Özet
In this work we investigated the role of Sn doping on mechanical and structural properties of Bi1.75Pb0.25Sr2Ca 2Cu3-xSnxO10+y (x = 0.0, 0.1, 0.3 and 0.5) superconducting ceramic material. All samples were fabricated with glass ceramic method. The prepared samples were characterized by using scanning electron microscope (SEM), energy dispersive spectroscopy (EDS), X-ray powder diffractometer (XRD) and static microhardness indenter. Surface morphology, orientation of grains, and elemental composition analysis of the samples were made by SEM and EDS measurements, respectively. Texturing and lattice parameters a and c were determined by XRD measurements. Load dependent and load independent microhardness, elastic modulus, yield strength and fracture toughness were obtained by hardness measurements. In this work we focused on Vickers microhardness measurements in order to characterize the mechanical properties of our samples. Experimental results of Vickers microhardness measurements were analyzed by using Meyer's law, the elastic/plastic deformation model, proportional sample resistance model (PSR), modified PSR model and Hays-Kendall (HK) approach. From these analyses, HK approach was determined as the most successful model describing the mechanical properties of our samples. Finally in this study, the changes on the mechanical and microstructural properties of Sn doped Bi-2223 superconductors and their possible reasons were also discussed in detail. © 2013 Springer Science+Business Media New York.
Anahtar Kelimeler
Makale Türü Özgün Makale
Makale Alt Türü SSCI, AHCI, SCI, SCI-Exp dergilerinde yayımlanan tam makale
Dergi Adı JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS
Dergi ISSN 0957-4522
Dergi Tarandığı Indeksler SCI
Makale Dili İngilizce
Basım Tarihi 11-2013
Cilt No 24
Sayı 11
Sayfalar 4270 / 4278
Doi Numarası 10.1007/s10854-013-1396-7
Makale Linki http://link.springer.com/10.1007/s10854-013-1396-7