Yazarlar |
Doç. Dr. Nesrin İÇLİ
Kastamonu Üniversitesi, Türkiye |
Özet |
Apple sour is a traditional product of Kastamonu, Turkey. It is consumed by spreading on bread or drinking after diluting with water. The aim of this study was to determine patulin (PAT) and 5-hydroxymethylfurfural (HMF) in apple sour. This study is the first to evaluate the occurrence of PAT and HMF in apple sour. The samples were extracted with ethyl acetate using liquid-liquid extraction technique. PAT and HMF were determined by HPLC with UV detection. PAT was detected in all samples, and the PAT level in 94.9% of samples was found to be equal or greater than the legal limit for juice concentrates. The mean value for PAT was found to be 284 ± 307 μg kg−1. PAT levels in 13 of 39 samples were in the range of 100 ≤ x < 200 μg kg−1, two samples were in the range of 0 ≤ x < 50 μg kg −1 and two samples were in the range of 1000 ≤ x < 1500 μg kg1. HMF levels of all samples were above the legal limit for solid molasses. The mean value for HMF was found to be 16215 ± 13317 mg kg−1. HMF levels of 10 of 39 samples were determined to be in the range of 10000 ≤ x < 20000 mg kg−1, eight samples were in the range of 20000 ≤ x < 30000 mg kg−1 and only three samples were in the range of 100 ≤ x < 1000 mg kg−1. There was a significant and inverse relationship between HMF and pH of the samples. These results indicate that consumption of apple sour is a considerable risk in terms of HMF and PAT toxicity. |
Anahtar Kelimeler |
apple sour | food safety | HMF | HPLC | Patulin |
Makale Türü | Özgün Makale |
Makale Alt Türü | SSCI, AHCI, SCI, SCI-Exp dergilerinde yayımlanan tam makale |
Dergi Adı | FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT |
Dergi ISSN | 1944-0049 |
Dergi Tarandığı Indeksler | SCI |
Dergi Grubu | Q2 |
Makale Dili | İngilizce |
Basım Tarihi | 01-2019 |
Cilt No | 36 |
Sayı | 6 |
Sayfalar | 952 / 963 |
Doi Numarası | 10.1080/19440049.2019.1605207 |
Makale Linki | http://dx.doi.org/10.1080/19440049.2019.1605207 |