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Processing, phase evaluation and mechanical properties of MoSi2 doped 4TaC-HfC based UHTCs consolidated by spark plasma sintering   
Yazarlar
Dr. Öğr. Üyesi Farzin ARİANPOUR Dr. Öğr. Üyesi Farzin ARİANPOUR
Kastamonu Üniversitesi, Türkiye
Farhad Golestanifard
Iran University of Science and Technology, Iran
Hamidreza Rezaie
Iran University of Science and Technology, Iran
Mehdi Mazaheri
National Institute for Materials Science, Japan
Ali Celik
Anadolu Üniversitesi, Turkey
Ferhat Kara
Anadolu Üniversitesi, Turkey
Gilbert Fantozzi
Matériaux : Ingénierie et science, France
Özet
In this research, binary 4TaC-HfC based composites were consolidated using carbide materials and addition of 0-15 vol.% MoSi2 by means of spark plasma sintering at 2000 °C. The nearly full dense and monophase specimens were fabricated with a relative density value higher than 99%. Mechanical tests revealed values of 18-19 GPa and 4-4.3 MPa·m1/2, for average Vickers hardness and fracture toughness of the composites, respectively. Analysis of linear shrinkage during densification revealed that MoSi2 addition increased densification rate and decreased the time required to reach full density at 2000 °C. It is proposed that at the intermediate stage of sintering, mass transfer can be accelerated by formation of a silicide based liquid phase and viscous flow mechanisms. The formation of binary 4TaC-HfC solid solution phase enhanced the densification process at the final stage of sintering.
Anahtar Kelimeler
Densification | Microstructure | Phase evolution | Spark plasma sintering | Tantalum hafnium carbide
Makale Türü Özgün Makale
Makale Alt Türü SCOPUS dergilerinde yayımlanan tam makale
Dergi Adı International Journal of Refractory Metals and Hard Materials
Dergi ISSN 0263-4368
Makale Dili İngilizce
Basım Tarihi 04-2016
Cilt No 56
Sayı 1
Sayfalar 1 / 7
Doi Numarası 10.1016/j.ijrmhm.2015.11.011