Effects of chelating agent on sol-gel synthesis of nano zirconia: The comparison of Pechini and sugar-based methods
Yazarlar (5)
Faramarz Kazemi Amirkabir University Of Technology, İran
Dr. Öğr. Üyesi Farzin ARİANPOUR Kastamonu Üniversitesi, Türkiye
Mahdiar Taheri The Australian National University, Avustralya
Ali Saberi Universität Bayreuth, Almanya
Hamid Reza Rezaie Iran University Of Science And Technology, İran
| Makale Türü | Özgün Makale (SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale) | ||
| Dergi Adı | International Journal of Minerals Metallurgy and Materials (Q4) | ||
| Dergi ISSN | 1674-4799 Wos Dergi Scopus Dergi | ||
| Dergi Tarandığı Indeksler | SCI | ||
| Makale Dili | İngilizce | Basım Tarihi | 01-2020 |
| Cilt / Sayı / Sayfa | 27 / 5 / 693–702 | DOI | 10.1007/s12613-019-1933-3 |
| Özet |
| This study focused on the comparison of the Pechini and sugar-based combustion synthesis methods to produce nano-zirconia. Zirconium hydroxide was utilized as metal precursor and citric acid, sucrose, and fructose were used as chelating agents, followed by calcination at 500, 600, and 700°C in air, respectively. Characterization was conducted by thermal analysis, specific surface area measurement, Fourier transform infrared spectroscopy, X-ray diffraction, and scanning and transmission electron microscopy. When sucrose and citric acid were used as chelating agents during synthesis, mixtures of monoclinic and tetragonal phases were formed after calcination at 600 and 700°C. In the fructose samples, the tetragonal structure was the unique characterized phase. The tetragonal parameters in the fructose samples were determined using the diffraction data and the lattice parameter ratio was proven to … |
| Anahtar Kelimeler |
| chelation | nanopowder | Pechini | sol-gel | sugar | zirconia |
BM Sürdürülebilir Kalkınma Amaçları
| Atıf Sayıları | |
| Scopus | 27 |
| Google Scholar | 31 |