Revival of quantum confinement effect and stabilization of tetragonal phase in TiO2 Nanopowders with annealing temperature
Yazarlar (4)
Doç. Dr. Elif AŞIKUZUN TOKEŞER Kastamonu Üniversitesi, Türkiye
U. Esturk
Kastamonu Üniversitesi, Türkiye
S. Kurnaz
Kastamonu Üniversitesi, Türkiye
Prof. Dr. Özgür ÖZTÜRK Kastamonu Üniversitesi, Türkiye
Makale Türü Özgün Makale (SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
Dergi Adı Journal of Materials Science Materials in Electronics (Q2)
Dergi ISSN 0957-4522 Wos Dergi Scopus Dergi
Dergi Tarandığı Indeksler SCI-Expanded
Makale Dili İngilizce Basım Tarihi 07-2025
Cilt / Sayı / Sayfa 36 / 19 / 1204–0 DOI 10.1007/s10854-025-15283-z
Makale Linki https://doi.org/10.1007/s10854-025-15283-z
Özet
This research is concerned with the variations of mechanical, structural, physical, and magnetic properties of titanium dioxide (TiO2) nanopowders produced via sol–gel method with annealing temperatures intervals 300 to 1100 °C. The effects of the phase transitions on the main chracteristics of TiO2 nanopowders are exstensively analyzed using X-ray diffraction (XRD), scanning electron microscopy (SEM), vibrating sample magnetometry (VSM), and Vickers microhardness (Hv) measurements. XRD investigations reveal an amorphous crystal structure at lower annealing temperatures (300–400 °C), followed by the formation of the chracteristic anatase phase (450–500 °C), and finally the transition to the rutile phase (600–1100 °C). All TiO2 nanopowders exhibit a tetragonal crystal structure. The avarage grain size parameter is found to increase depending on the lattice strain relaxation while dislocation density …
Anahtar Kelimeler
BM Sürdürülebilir Kalkınma Amaçları
Atıf Sayıları
Web of Science 3
Scopus 3
Google Scholar 4
Revival of quantum confinement effect and stabilization of tetragonal phase in TiO2 Nanopowders with annealing temperature

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