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Revival of quantum confinement effect and stabilization of tetragonal phase in TiO2 Nanopowders with annealing temperature  
Yazarlar (1)
S Kurnaz
Kastamonu Üniversitesi, Türkiye
Devamını Göster
Özet
This research is concerned with the variations of mechanical, structural, physical, and magnetic properties of titanium dioxide (TiO 2) nanopowders produced via sol--gel method with annealing temperatures intervals 300 to 1100 C. The effects of the phase transitions on the main chracteristics of TiO 2 nanopowders are exstensively analyzed using X-ray diffraction (XRD), scanning electron microscopy (SEM), vibrating sample magnetometry (VSM), and Vickers microhardness (H v) measurements. XRD investigations reveal an amorphous crystal structure at lower annealing temperatures (300--400 C), followed by the formation of the chracteristic anatase phase (450--500 C), and finally the transition to the rutile phase (600--1100 C). All TiO 2 nanopowders exhibit a tetragonal crystal structure. The avarage grain size parameter is found to increase depending on the lattice strain relaxation while dislocation density ...
Anahtar Kelimeler
Makale Türü Özgün Makale
Makale Alt Türü Uluslararası alan indekslerindeki dergilerde yayınlanan tam makale
Dergi Adı Journal of Materials Science: Materials in Electronics
Dergi Tarandığı Indeksler
Makale Dili İngilizce
Basım Tarihi 07-2025
Cilt No 36
Sayı 19
Sayfalar 1 / 21
BM Sürdürülebilir Kalkınma Amaçları
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